By J. Lawrynowicz, J. Lodz
Textual content: English, French
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Extra resources for Analytic Functions, Blazejewko 1982
For each source of phospholipids, special standards are needed due to the different distribution of fatty acids. These standards are expensive and in some cases are not available. Another problem is represented by the analysis of phospholipids in complex matrices. In many cases, separation is impossible or very difficult, not least due to the surface activity, which is desired in the application of phospholipids, but which complicates the analysis of these compounds. Therefore, a method is needed which is selective in the detection of phospholipids in order to avoid a separation from the matrix.
The details of this technique and fbrther applications will be discussed in the section NMR in body fluids. 1 Analysis of Single Drugs in Dosage Forms The characterization of drugs in dosage forms by means of NMR spectroscopy is an interesting goal, because the identity and quantity can be determined simultaneously. Hanna et al.  describe a method for analysis of chlorpheniramine maleate in tablets and injection. After extraction of the drug, an internal standard (tert-butanol) is added and a 90-MHz spectrum is recorded.
N CH, 38 Analysis of Drugs N ifed ipine dL. , 15 . 10 , , T T - 05 GO Figure 3-27: 'H NMR spectrum of nifedipine, 300 MHz, solvent methanol-d4, "SSL" L.. 0 m-... 5 I . . 10 , I . 5 . , , I 00 Figure 3-28: 'H NMR spectrum of nifedipine after photo-oxidation, 300 MHz, solvent methanol-d4,"SSL" B. K. DiehI and U. Holzgrabe 39 Fluoroquinolone compounds bearing a fluorine atom in position 6 and mostly a piperazine ring in position 7 attract interest as potent antibacterials. They are known to decompose upon irradiation, resulting in products which do not have any antibacterial activity, but show photosensitization properties in vivo.
Analytic Functions, Blazejewko 1982 by J. Lawrynowicz, J. Lodz